الطباقية الحياتية لمتحجرات النانو في حد التماس مابين تكويني كوميتان وشرانش وادي جقجق السليمانية شمال شرق العراق

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1 NANNOFOSSILS BIOZONES OF CONTACT BETWEEN KOMETAN AND SHIRANISH FORMATIONS, CHAQCHAQ VALLEY, SULAIMANYIA, NE IRAQ Omar Ahmed Al-Badrani 1 Kamal H. Karim 2 and Khalid M Ismail 3 Key words: Shiranish Formation, Kometan Formation, gradational contact, transitional zone, nannofossils, Chaqchaq valley. ABSTRACT Nineteen species of calcareous nannofossils were identified from contact between Kometan and Shiranish Formations that exposed in the Chaqchaq valley northwest of the Sulaimanyia city, NE Iraq. The recorded calcareous nannofossils assemblages permit recognition of two biozones: 2- Ceratolithoides aculeus Interval Biozone (CC 20) 1-Aspidolithus parcus Calculites ovalis Interval Biozone (CC 18- CC19) Based on nannofossils biozonation, the contact between Kometan and Shiranish Formations is considered to be conformable. In the studied area, the age of the Shiranish Formation is extending into Early Campanian. الطباقية الحياتية لمتحجرات النانو في حد التماس مابين تكويني كوميتان وشرانش وادي جقجق السليمانية شمال شرق العراق " " عمر احمد البدراني كمال حاجي كريم و خالد محمود اسماعيل كوميتاس ششارانا الم كشا س وا شا ماسنين تكاو الكلسية من حد التماس " " النانو شخص تسعة عشر نوع من متحجرات مكان تمييان نطاسقين حياستيين السليمسنية شمسل شرق العراق. خالل االنتشسر الطبسق لحشو المتحجرات جقجق شمسل غرب مد ة همس: 2- Ceratolithoides aculeus Interval Biozone (CC 20) 1-Aspidolithus parcus Calculites ovalis Interval Biozone (CC 18- CC19) اعتمس ا على المتحجرات المت سهية الصغر شجد ا شرانا من الكسمبسنيس المبكر و الم طقة الدراسة. حد التمس مسنين تكو كوميتس ششرانا متواوق. ش متد عمار تكاو ن 9 Assistant professor Dept. of Geology, College of Science, Mosul University, Mosul, Iraq. 2 Professor Dept. of Geology, College of Science, Sulamani University, Sulaimanyiah, Iraq. karimgeology@yahoo.com 3 Assistant Professor Dept. of Geology, College of Science, Sulamani University, Sulaimaniyiah, Iraq. khalshin@yahoo.com 91

2 Nannofossils biozones of the contact between Kometan and Shiranish formations, Omer A. Al Badrani, Iraqi Bulletin al of Geology and Mining Vol.8, No.1,2012 INTRODUCTION Kometan Formation is first described by Dunnington (1953, in Bellen et al., 1959). It is exposed in High and Low Folded Zones in subsurface sections in the Mesopotamian Zone (Dunnington9191; Buday, 1980, Buday and Jassim, 1987). The type section is located at 400m to the west of Kometan village in the Naudasht valley in the foothills of Qandil Mountain about 20 km to the north of Ranyia town in the Imbricated Zone (Fig.1). According to aforementioned authors, the formation is composed of well bedded, light grey or white limestone. It contains locally chert nodules or ribbons with rare pyrite concretions. The thickness of the formation, in the High Folded and Imbricated Zones, reaches ( ) m. The lower and upper contacts of the formation are unconformable (Dunnington, 1953 in Bellen et al., 1959, Buday, 1980 and Al-Khafaf, 2005). The first author added that faunal and intense glauconization indicate depositional hiatus and probable erosion. In this contact, in addition to glauconite and faunal break, he found polygenetic micropebbles. Recent sedimentological studies such as Karim, et al. (2008) and Taha (2008) analyzed what called by Bellen et al., 1959 polygenetic micropebbles. They proved that there are no such deposits in all six studied sections. In the contact, they found siliceous nodules and glauconite at one section. In the other section, they observed gradational contact as regular alternation of white limestone and bluish white marl. Shiranish Formation is the most important rock unit throughout the Cretaceous of north Iraq. It s type section is first described by Henson, 1940 (cited in Bellen et al., 1959) and lies at Shiranish Islam Village near Zakho City. It reaches about 8 meters in thickness and consists mainly of marl and marly limestone representing off shore, open sea sediments of the Late Campanian- Maastrichtian age on the basis of the foraminiferal assemblages content. LOCATION AND GEOMORPHOLOGY The section is located 10km to northwest of Sulaimaniyah city and about 3 km south of Lower Hanaran Village in the middle part of the Chaqchaq valley. It is located in the intersection of latitude 35 o 39 ' 46 " N and longitude 45 o ' 35 " E (Fig.1 and 2). The contact is exposed clearly along the right bank (when looks upstream) of the perennial Chaqchaq stream (Fig.3). The Chaqchaq valley is flat bottomed at its mouth, to the east of Sulaimanyia city while it become v-shaped at it's middle part and head. The valley is surrounded from southwest, north and northeast by Piramagroon, Daban and Azmir Mountains respectively (Fig.2). Structurally, it consists of wide syncline in which Tanjero, Shiranish and Kometan Formations are exposed near the it's axis and along the lower parts of the limbs. Along the upper parts of southwestern and northeastern limbs; Qamchuqa and Balambo Formations are exposed respectively. MATERIAL AND METHODOLOGY Forty one samples are taken from the Kometan and Shiranish Formations across the contact between them. Two samples are taken from proper Kometan Formation at the base of the sampled interval. Eight samples are taken from what it seems to be the transition Zone (alternation between white pelagic limestone and bluish marl) at the middle part of the sampled intervals. The other samples are taken from the proper Shiranish Formation (bluish white marl) at the top of the sampled intervals. These samples are inspected under normal and polarized microscope with more than 1000 magnifications. The samples are identified and the significant samples were photographed and then systematic paleontology and biozonation are achieved as mentioned hereinafter. For preparing smear slides, a small part of the sample is put on a glass slide and mixed thoroughly with distilled water. The slide is dried on a hot plate and covered with glass cover slide by using Canada balsam and examined with normal microscope.

3 Fig.1: Google earth view of the area around the sampled section in the Chaqchaq valley. Fig.2: Geological map of the area around Sulaimaniyia city includes Chachaq stream (modified from Sissakian, 2000 and Ali, 2009) 29

4 Nannofossils Iraqi Bulletin biozones of Geology of the and contact Mining between Kometan and Shiranish Vol.8, No.1,2012 formations, Omer A. Al Badrani, et al Fig. 3: Gradational contact between Kometan and Shiranish formations in the Chaqchaq stream. The contact is represented by alternation of grey marl and fine crystalline limestone. The marl increases towards Shiranish Formation. SYSTEMATIC PALEONTOLOGY The following species are identified and classified below: Kingdom Protista Division Chrysophyta Class Coccolithophyceae Family Arkhangelskiellaceae Bukry, 1969 Genus Aspidolithus Noël, 1969 Aspidolithus parcus (Stradner, 1963) Noël, 1969 (Figs. 4.1,2) Aspidolithus sp. (Fig. 4.3) Family Calyptrosphaeraceae Boudreaux and Hay, 1969 Genus Lucianorhabdus Deflandre, 1959 Lucianorhabdus cayeuxii Deflandre, 1959 (Fig. 4.16) Family Chiastozygaceae Rood, Hay and Barnard, 1973 Genus Calculites Prins and Sissingh, 1977 Calculites obscurus (Deflandre, 1959) Prins and Sissingh, 1977 (Fig. 4.5) Calculites ovalis (Stradner, 1963) Prins and Sissingh, 1977(Fig. 4.6) Family Chiastozygaceae Rood, Hay and Barnard, 1973 Genus Chiastozygus Gartner, 1968 Chiastozygus platyrhethum Hill, 1976 (Fig. 4.10) Chiastozygus sp. (Fig. 4.11) Family Eiffellithaceae Reinhardt, 1965 Genus Eiffellithus Reinhardit, 1965 Eiffellithus eximius (Stover, 1966) Perch-Nielsen, 1968 (Figs. 4.12,13) Eiffellithus turriseffelii (Deflandre, 1954) Reinhardit, 1965 (Fig. 4.14)

5 Family Ellipsagelosphaeraceae Noël, 1965 Genus Watznaueria Reinhardt, 1964 Watznaueria barnesae (Black, 1959) Perch-Nielsen, 1968 (Fig. 4.21) Watznaueria biporta Bukry, 1969 (Fig. 4.) Family Nannoconceae Deflandre, 1959 Genus Nannoconus Kamptner Nannoconus malticadus Deflandre and Deflandre, 1959 (Fig. 4.19) Family Podrorhabdaceae Noel, 1965 Genus Bipodorhabdus Noël, 1970 Bipodorhabdus tesselatus Noël, 1970 (Fig. 4.4) Family Polycyclolithaceae Forchheimer, 1972 Genus Micula Vekshina, 1959 Micula decussata Vekshina, 1959 (Fig. 4.17) Micula swastica (Fig. 4.18), Stradner and Steinmetz, 1984 Genus Lithastrinus Stradner, 1962 Lithastrinus grillii Stradner, 1962 )Fig ( Family Zygodiscaceae Hay and Mohler, 1967 Genus Reinhardites Perch-Nielsen, 1968 Reinhardites anthrophorus (Deflandre, 1959) Perch-Nielsen, 1968 (Fig. 4.20) Incertae sedis Genus Ceratolithoides Bramlette and Marini, 1964 Ceratolithoides verbeekii Perch-Nielsen, 1979 (Figs. 4.8,9) Ceratolithoides aculeus (Stradner, 1961) Prins and Sissingh, 1977 (Fig. 4.7) NANNOBIOSTRATIGRAPHY The boistratigraphic subdivision of the section is achieved which resulted in two main interval zone as shown in the below and in the Fig.5. 1-Aspidolithus parcus Calculites ovalis Interval Biozone (CC 18- CC19) Definition: First occurrence of Aspidolithus parcus to first occurrence of Ceratolithoides aculeus. Thickness: 24.5 meter of limestone, marly limestone and marl. Boundaries and Discussion: Perch-Nielsen (1977) used the same definition for her Early Campanian Eiffellithus eximius Zone. Verbeek (1977), Roth(1978) and Doeven(1983) defined a Broinsonia parca Zone from the first occurrence of Broinsonia parca to first occurrence Ceratolithoides aculeus, the event used by Sissingh (1977) to define the top of his zone CC19 (Perch-Nielsen, 1985), therefore the age of this biozone is Early middle Campanian (Gradstein et al., 2004).

6 Nannofossils Iraqi Bulletin biozones of Geology of the and contact Mining between Kometan and Shiranish Vol.8, No.1,2012 formations, Omer A. Al Badrani, et al Fig.4: Nannofossils found in the sampled section across the boundary between Kometan and Shiranish formations). (The names of the species are listed in page 25)

7 1, 2) Aspidolithus parcus (Stradner, 1963) Noël, 1969, sample no.2, normal and polarized transmitted light. 3) Aspidolithus sp. sample no.18, normal transmitted light. 4) Bipodorhabdus tesselatus Noël, 1970, sample no.2, normal transmitted light. 5) Calculites obscurus(deflandre, 1959) Prins and Sissingh, 1977, sample no.6, polarized transmitted light. 6) Calculites ovalis (Stradner, 1963) Prins and Sissingh, 1977, sample no.2, polarized transmitted light. 7) Ceratolithoides aculeus (Stradner, 1961) Prins and Sissingh, 1977 sample no.18, normal transmitted light. 8, 9) Ceratolithoides verbeekii Perch-Nielsen, 1979, sample no.6, normal and polarized transmitted light. 10) Chiastozygus platyrhethum Hill, 1976 sample no.23, normal transmitted light. 11) Chiastozygus sp. sample no.18, normal transmitted light. 12, 13) Eiffellithus eximius (Stover, 1966) Perch-Nielsen, 1968, sample no.11, normal and polarized transmitted light. 14) Eiffellithus turriseffelii (Deflandre, 1954) Reinhardit, 1965, sample no.18, polarized transmitted light. 15) Lithastrinus grillii Stradner, 1962, sample no.11, polarized transmitted light. 16) Lucianorhabdus cayeuxii Deflandre, 1959, sample no.8, polarized transmitted light. 17) Micula decussata Vekshina, 1959, sample no.10, normal transmitted light. 18) Micula swastica Stradner and Steinmetz, 1984, sample no.6, polarized transmitted light. 19) Nannoconus malticadus Deflandre and Deflandre, 1959, sample no.9, polarized transmitted light. 20) Reinhardites anthrophorus (Deflandre, 1959) Perch-Nielsen, 1968, sample no.10, normal transmitted light. 21) Watznaueria barnesae (Black, 1959) Perch-Nielsen, 1968, sample no.9, polarized transmitted light. )Watznaueria biporta Bukry, Sample no.2, polarized transmitted light. 29

8 Nannofossils biozones of the contact between Kometan and Shiranish formations, Omer A. Iraqi Al Badrani, Bulletin of et Geology al and Mining Vol.8, No.1,2012 Fig.5: Range chart of the nannofossils that are found in the sampled section across the boundary between Kometan and Shiranish Formations

9 2- Ceratolithoides aculeus Interval Biozone (CC 20) Definition: First occurrence of Ceratolithoides aculeus to first occurrence of Quadrum sissinghi. Thickness: 16 meter marl. Boundaries and Discussion: Roth (1978) define the Tetralithus aculeus zone from the first occurrence of Tetralithus aculeus to the first occurrence of Tetralithus trifidus including CC20 and CC21 (Perch-Nielsen, 1985), in the present study the Quadrum sissinghi not singed therefore unable to determined the upper boundary of the biozone, but the age of this biozone is Middle Campanian (Gradstein et al., 2004). DISCUSSION Two results are important in this study: The first is gradational contact which has representative sediments as indicated by the recorded nannofossils. The second is that the boundary between the two formations is located in the Early Campanian instead of Middle Campanian (as mentioned previously). The biostratigraphically proved gradational boundary (conformable contact) is the first detail one. This proof has great paleogeographic and tectonic important which change the previous idea about uplift and subsidence in the Middle Campanian. Conversely, the study shows more calm tectonics and different paleogeographic setting of the northeastern Iraq during Campanian and Maastrichtian. Recent sedimentological study discussed nine sections in Sulaimanyia and Erbil vicinity and in all these sections, it is inferred that there are submarine erosion or slow rate of the sedimentation (represented by glauconitic bed) in two nearby sections in Dokan area (see Karim, et al., 2008 and Taha, 2008). The authors showed that the contact in other sections is gradational and without occurrence of conglomerate, erosional surface, paleosoil and glauconite beds. The only fulfillment lack of these papers was the paleontological proof which is provided by the present study. The occurrence of the contact in the Early Campanian is more or less abnormal, as the previous studies indicated that the Middle Campanian is missing due to uplift of the area and then starting of erosion by which polygenetic micropebbles are deposited (Buday, 1980 and Bellen et al., 1959) and then Shiranish Formation is deposited in Late Campanian. According to Jassim and Goff (2006), Al Jassim et al. (1989) and Al-Khafa (2005) Kometan Formation extends from Turonian to Middle Campanian. The same authors assigned that the age of the Shiranish Formation is Late Campanian- Maastrichtian. This age of Kometan and Shiranish Formations (in the studied area) is new. In the literature, there is one indirect pointing to the possibility of this age. This is proved in the sedimentological study of Taha (2008) who correlated the glauconite bed in Dokan area with same bed in the north of the Sulaimanyia city. He showed that the galuconite bed at Dokan Area is located nearly at contact between the two formations while it is located inside the Shiranish Formation (30 m above the contact) (Fig.6) in the north of Sulaimanyia city section. As the glauconite beds has wide distribution (Glaway,1988; Vail et al. 1977; Loutit et al. 1988; Haq,1991; Emery and Myers, 1996), therefore, the bed most possibly has the same age in both areas and thus both sedimentology and biozonation has more or less same result as concerned to the contact in Sulaimanyia area.

10 Nannofossils biozones of the contact between Kometan and Shiranish formations, Omer A. Iraqi Al Badrani, Bulletin et of al Geology and Mining Vol.8, No.1,2012 Fig.6: Sedimentological correlation between the glauconite beds near the boundary between Kometan and Shiranish formations in the lower Dokan and Kani Bardina sections (7 kms to northeast of Sulaimaniyah city). It shows that in the latter section, the bed located inside Shiranish Formation (Taha, 2008). CONCLUSIONS This study has the following conclusions: The recorded calcareous nannofossils assemblages permit the recognition of two biozones: 1-Aspidolithus parcus Calculites ovalis Interval Biozone (CC 18- CC19) 2- Ceratolithoides aculeus Interval Biozone (CC 20) This study inferred that the contact between Kometan and Shiranish Formations is conformable with Early Campanian age. The contact age of the Shiranish Formation extends to Early Campanian. 21

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